"Raw data belong to: Mikucki, EE, Lockwood, BL (2021) Local thermal environment and warming influence supercooling and drive widespread shifts in the metabolome of diapausing Pieris rapae butterflies. Journal of Experimental Biology. doi:10.1242/jeb.243118" "Metadata for sheet ""Mikucki_Lockwood_JEB_2021_Raw_Metabolomics_NegativeMode"" " Column Entry Value Unit Explanation A Feature ID Numerical Metabolite identification number B row m/z Numerical Kg/C Mass to charge ratio used to determine molecular weight C row retention time Numerical Minutes Mass spec timing D 1[VT_C_4]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 75 individual E 2[VT_C_5]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 25 individual F 3[VT_C_6]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 75 individual G 4[VT_C_9]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 25 individual H 5[VT_C_10]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 75 individual I 6[VT_C_11]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 50 individual J 7[VT_C_14]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 75 individual K 8[VT_C_16]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 25 individual L 9[VT_C_19]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 50 individual M 10[VT_C_22]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 25 individual N 11[VT_C_24]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 25 individual O 12[VT_C_26]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 75 individual P 13[VT_C_27]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 25 individual Q 14[VT_C_29]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 75 individual R 15[VT_C_30]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 50 individual S 16[VT_C_32]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 50 individual T 17[VT_C_34]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 50 individual U 18[VT_LTC_1]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 75 individual V 19[VT_LTC_2]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 25 individual W 20[VT_LTC_4]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 75 individual X 21[VT_LTC_9]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 25 individual Y 22[VT_LTC_14]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 25 individual Z 23[VT_LTC_15]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 50 individual AA 24[VT_LTC_16]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 75 individual AB 25[VT_LTC_20]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 75 individual AC 26[VT_LTC_21]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 75 individual AD 27[VT_LTC_23]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 50 individual AE 28[VT_LTC_25]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 75 individual AF 29[VT_LTC_29]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 25 individual AG 30[VT_LTC_30]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 25 individual AH 31[VT_LTC_31]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A or a Vermont Chronic Warming Day 25 individual AI 32[VT_LTC_33]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 50 individual AJ 33[VT_LTC_34]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 25 individual AK 34[VT_LTC_35]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 50 individual AL 1[pooled_Control]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for pooled Control samples AM 1[pooled_LTW]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for pooled Chronic Warming samples "Metadata for sheet ""Mikucki_Lockwood_JEB_2021_Raw_Metabolomics_PositiveMode"" " Column Entry Value Unit Explanation A Feature ID Numerical Metabolite identification number B row m/z Numerical Kg/C Mass to charge ratio used to determine molecular weight C row retention time Numerical Minutes Mass spec timing D 1[VT_C_4]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 75 individual E 2[VT_C_5]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 25 individual F 3[VT_C_6]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 75 individual G 4[VT_C_9]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 25 individual H 5[VT_C_10]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 75 individual I 6[VT_C_11]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 50 individual J 7[VT_C_14]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 75 individual K 8[VT_C_16]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 25 individual L 9[VT_C_19]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 50 individual M 10[VT_C_22]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 25 individual N 11[VT_C_24]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 25 individual O 12[VT_C_26]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 75 individual P 13[VT_C_27]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 25 individual Q 14[VT_C_29]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 75 individual R 15[VT_C_30]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 50 individual S 16[VT_C_32]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 50 individual T 17[VT_C_34]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Control Day 50 individual U 18[VT_LTC_1]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 75 individual V 19[VT_LTC_2]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 25 individual W 20[VT_LTC_4]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 75 individual X 21[VT_LTC_9]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 25 individual Y 22[VT_LTC_14]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 25 individual Z 23[VT_LTC_15]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 50 individual AA 24[VT_LTC_16]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 75 individual AB 25[VT_LTC_20]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 75 individual AC 26[VT_LTC_21]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 75 individual AD 27[VT_LTC_23]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 50 individual AE 28[VT_LTC_25]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 75 individual AF 29[VT_LTC_29]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 25 individual AG 30[VT_LTC_30]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 25 individual AH 31[VT_LTC_31]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A or a Vermont Chronic Warming Day 25 individual AI 32[VT_LTC_33]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 50 individual AJ 33[VT_LTC_34]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 25 individual AK 34[VT_LTC_35]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for a Vermont Chronic Warming Day 50 individual AL 1[pooled_Control]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for pooled Control samples AM 1[pooled_LTW]n.mzXML Peak height Numerical Integrated peak height Integrated peak height for metabolite features in column A for pooled Chronic Warming samples "Metadata for sheet ""Mikucki_Lockwood_JEB_2021_SCP_Populations""" Column Entry Value Unit Explanation A Population Categorical Vermont; North Carolina Population origin of Pieris rapae pupae B Treatment Categorical Control Warming treatment C Day Categorical 25; 50; 75 Day in the experiment when supercooling point was measured D Weight Numerical Grams Indiivudal pupal weight measured immediately before supercooling point analysis E Supercooling point (SCP) Numerical Degrees Celcius Internal freezing temperature "Metadata for sheet ""Mikucki_Lockwood_JEB_2021_SCP_Warming_Treatments""" Column Entry Value Unit Explanation A Population Categorical Vermont Population origin of Pieris rapae pupae B Treatment Categorical Control; Chronic Warming; Acute Warming Warming treatments C Day Categorical 25; 50; 75 Day in the experiment when supercooling point was measured and individuals were subsequently frozen and kept at -80¡C until metabolimics analysis. D Weight Numerical Grams Individual pupal weight mesaured immediately before supercooling point analysis E Supercooling point (SCP) Numerical Degrees Celcius Internal freezing temperature