CLOSED Version 2.0 Language English Run 8 RunSerial 580 Instrument SDT Q600 V8.3 Build 101 Module DSC-TGA Standard InstSerial 0600-0291 Operator KR File \\Universi-ecd1c7\ta\Data\SDT\Elham\Fe-03-Spent-Air_010219.001 Sample Fe 0.3 Spent Size 17.8910 mg ProcName Ramp Method Ramp Comment Ramp from RT to 900°C at 10°C/min in Air Xcomment Pan: Alumina Xcomment Gas1: Air 100.0 ml/min Xcomment Gas2: Air 0.0 ml/min Text Exotherm Up Kcell 0.926000 InstCalDate Weight: 2018-11-21 Time: 10:36:44 TempRange 200.05 to 1392.64 °C InstCalFile Weight: \\Universi-ecd1c7\ta\Data\SDT\SDT TA Service\SDT Cal Nov 2018- after new beams fitted\SDT-WeightCal-Empty beams.001 InstCalDate Heat Flow: 2018-11-21 Time: 15:15:56 TempRange 200.09 to 1386.13 °C InstCalFile Heat Flow: \\Universi-ecd1c7\ta\Data\SDT\SDT TA Service\SDT Cal Nov 2018- after new beams fitted\DSCHeatFlow-EmptyCrucibles.001 InstCalDate DTA Baseline: 2005-12-02 Time: 11:12:42 TempRange 304.42 to 1487.52 °C InstCalFile DTA Baseline: \\D8stvp1j\ta\Data\SDT\TA Service\Installation 01-12-2005\TGA Empty Beams.001 TempCal 1 pts 423.49 419.53 Controls Gas 1 Event OFF Sampling 0.5 sec/pt AutoAnalysis Off MacroFile Nsig 4 Sig1 Time (min) Sig2 Temperature (°C) Sig3 Weight (mg) Sig4 Heat Flow (mW) Date 2019-02-01 Time 12:06:24 OrgMethod 1: Ramp 10.00 °C/min to 900.00 °C OrgFile C:\TA\Data\SDT\Elham\Fe-03-Spent-Air_010219.001 StartOfData .001400000 17.32797 17.89085 -30.14157 .004333333 17.35577 17.89012 -30.11133 0.01266666 17.38238 17.88959 -30.10926 0.02100000 17.41105 17.88942 -30.10572 0.02933333 17.44019 17.88884 -30.10086 0.03766667 17.46366 17.88808 -30.09457 0.04600000 17.48930 17.88774 -30.08683 0.05433334 17.51697 17.88742 -30.07774 0.06266666 17.54165 17.88664 -30.06744 0.07100000 17.56768 17.88602 -30.05584 0.07933334 17.60114 17.88610 -30.04278 0.08766666 17.62545 17.88644 -30.02930 0.09600000 17.64973 17.88623 -30.01632 0.1043333 17.67618 17.88596 -30.00367 0.1126666 17.70796 17.88617 -29.99061 0.1210000 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