Data from: Compatibilization of immiscible polymer blends through pendant ionic interactions
Data files
Jul 22, 2025 version files 12.13 MB
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Figures.zip
12.10 MB
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README.md
25.82 KB
Abstract
This dataset accompanies the article "Compatibilization of Immiscible Polymer Blends through Pendant Ionic Interactions" by Jerrick Edmund, Kseniia M. Karnaukh, Shuyi Xie, Elizabeth A. Murphy, Allison Abdilla, Eiko Ino, Javier Read de Alaniz, Craig J. Hawker, and Rachel A. Segalman. The article demonstrates the compatibilization of immiscible poly(dimethylsiloxane) and poly(n-butyl acrylate) mixtures through the introduction of sparse pendant ionic interactions, and probes the effect of charge density on the physical properties of the compatibilized blends. This dataset contains the necessary experimental data to reproduce all the figures in the main text and supporting information. Small angle X-ray scattering patterns, small-amplitude oscillatory shear rheological curves, nuclear magnetic resonance spectra, size-exclusion chromatograms, Fourier-transform infrared spectra, and differential scanning thermograms are included.
This README.txt file was generated on 2025-05-27 by JERRICK EDMUND
GENERAL INFORMATION
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Title of Dataset: Compatibilization of Immiscible Polymer Blends through Pendant Ionic Interactions
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Author Information
A. Principal Investigator Contact Information
Name: Rachel A. Segalman
Institution: University of California, Santa Barbara
Address: Materials Research Laboratory, University of California, Santa Barbara, 93106
Email: segalman@ucsb.eduB. Principal Investigator Contact Information
Name: Craig J. Hawker
Institution: University of California, Santa Barbara
Address: Materials Research Laboratory, University of California, Santa Barbara, 93106
Email: hawker@mrl.ucsb.eduC. Associate or Co-investigator Contact Information
Name: Jerrick Edmund
Institution: University of California, Santa Barbara
Address: Department of Chemical Engineering, University of California, Santa Barbara, 93106
Email: jedmund@ucsb.eduD. Associate or Co-investigator Contact Information
Name: Kseniia M. Karnaukh
Institution: University of California, Santa Barbara
Address: Department of Chemistry and Biochemistry, University of California, Santa Barbara, 93106
Email: kkarnaukh@ucsb.eduE. Associate or Co-investigator Contact Information
Name: Shuyi Xie
Institution: University of California, Santa Barbara
Address: Materials Research Laboratory, University of California, Santa Barbara, 93106
Email: shuyixie@ucsb.eduF. Associate or Co-investigator Contact Information
Name: Elizabeth A. Murphy
Institution: University of California, Santa Barbara
Address: Department of Chemistry and Biochemistry, University of California, Santa Barbara, 93106
Email: emurphy@ucsb.eduG. Associate or Co-investigator Contact Information
Name: Allison Abdilla
Institution: University of California, Santa Barbara
Address: Department of Chemistry and Biochemistry, University of California, Santa Barbara, 93106
Email: aabdilla@chem.ucsb.eduH. Associate or Co-investigator Contact Information
Name: Eiko Ino
Institution: University of California, Santa Barbara
Address: Materials Research Laboratory, University of California, Santa Barbara, 93106
Email: eiko_ino@ucsb.eduI. Associate or Co-investigator Contact Information
Name: Javier Read de Alaniz
Institution: University of California, Santa Barbara
Address: Department of Chemistry and Biochemistry, University of California, Santa Barbara, 93106
Email: jalaniz@ucsb.edu -
Date of data collection (single date, range, approximate date) 2023-01-01 to 2024-08-01
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Geographic location of data collection: Santa Barbara, CA
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Information about funding sources that supported the collection of the data: This work was supported by the National Science Foundation through the Materials Research Science and Engineering Center (MRSEC) at UC Santa Barbara: NSF DMR–2308708 (IRG-1). The research reported here made use of the shared facilities of the Materials Research Science and Engineering Center (MRSEC) at UC Santa Barbara: NSF DMR–2308708. The UC Santa Barbara MRSEC is a member of the Materials Research Facilities Network (www.mrfn.org). This work made use of facilities supported by an NSF Major Research Instrumentation award, MRI-1920299, for magnetic resonance instrumentation; and BioPACIFIC Materials Innovation Platform of the National Science Foundation under award No. DMR-1933487, for X-ray scattering instrumentation.
SHARING/ACCESS INFORMATION
- Licenses/restrictions placed on the data: N/A
- Links to publications that cite or use the data:
- Links to other publicly accessible locations of the data: N/A
- Links/relationships to ancillary data sets: N/A
- Was data derived from another source? No
- Recommended citation for this dataset:
DATA & FILE OVERVIEW
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File List: Files are organized into folders based on figure/table number from the corresponding manuscript and supporting information. Files are named as "Figure#_SampleID.csv"
A. Figure3: Small angle X-ray scattering patterns of (a) 1.0 mol% blend, and (b) 6.5 mol% blend at room temperature.
a. Figure3a_1molblend.csv
1. Variables: Scattering Wavevector [A-1], Intensity [arb. units]
2. Column names: q (A-1), I (arb. units)
b. Figure3b_6halfmolblend.csv
1. Variables: Scattering Wavevector [A-1], Intensity [arb. units]
2. Column names: q (A-1), I (arb. units)B. Figure4: Small angle X-ray scattering patterns of (a) 1.0 mol% blend at room temperature (RT), 150 C, and room temperature upon cooling; and (b) domain sizes of 1.0 mol% blend as a function of temperature.
a. Figure4a_1molblendVT.csv
1. Variables: Scattering Wavevector [A-1], Intensity [arb. units]
2. Column names: q_RT (A-1), I_RT (arb. units), q_150C (A-1), I_150C (arb. units), q_RT_cool (A-1), I_RT_cool (arb. units)
b. Figure4b_1molblendVTdomain.csv
1. Variables: Temperature [°C], Primary Peak Wavevector [A-1], Domain Size [nm]
2. Column names: T (°C), q* (A–1), d (nm)C. Figure5: Small-amplitude oscillatory shear rheological master curves of (a) 1.0 mol% blend and its parent polymers, and (b) 6.5 mol% blend and its parent polymers constructed by time-temperature superposition, and corresponding shift factors for (c) 1.0 mol% blend and its parent polymers, and (d) 6.5 mol% blend and its parent polymers.
a. Figure5a_1molmastercurves.csv
1. Variables: Reduced Frequency [rad/s], Storage Modulus [Pa], Loss Modulus [Pa]
2. Column names: waT_PnBA_SO3H (rad/s), G'_PnBA_SO3H (Pa), G''_PnBA_SO3H (Pa), waT_PDMS_Im (rad/s), G'_PDMS_Im (Pa), G''_PDMS_Im (Pa), waT_Blend (rad/s), G'_Blend (Pa), G''_Blend (Pa)
b. Figure5b_6halfmastercurves.csv
1. Variables: Reduced Frequency [rad/s], Storage Modulus [Pa], Loss Modulus [Pa]
2. Column names: waT_PnBA_SO3H (rad/s), G'_PnBA_SO3H (Pa), G''_PnBA_SO3H (Pa), waT_PDMS_Im (rad/s), G'_PDMS_Im (Pa), G''_PDMS_Im (Pa), waT_Blend (rad/s), G'_Blend (Pa), G''_Blend (Pa)
c. Figure5c_1molshiftfactors.csv
1. Variables: Temperature – Reference Temperature [°C], Log(Shift Factor) [unitless]
2. Column names: T-Tref_PnBA_SO3H (°C), log(aT)_PnBA_SO3H, T-Tref_PDMS_Im (°C), log(aT)_PDMS_Im, T-Tref_Blend (°C), log(aT)_Blend
d. Figure5c_6halfmolshiftfactors.csv
1. Variables: Temperature – Reference Temperature [°C], Log(Shift Factor) [unitless]
2. Column names: T-Tref_PnBA_SO3H (°C), log(aT)_PnBA_SO3H, T-Tref_PDMS_Im (°C), log(aT)_PDMS_Im, T-Tref_Blend (°C), log(aT)_BlendD. FiguresS1-2,S4-8,S13-14,S16-21,S23-26,S28-31,S33,S37-40: Nuclear magnetic resonance (NMR) spectra of synthesized small molecules, polymers, and blends.
a. FigureS1_PDMS1PVMS.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
b. FigureS2_PDMS7PVMS.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
c. FigureS4_ImCl.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
d. FigureS5_ImSH.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
e. FigureS6_PDMS1Im.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
f. FigureS7_PDMS6halfIm.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
g. FigureS8_PDMS6halfImCOSY.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Row 1 and Column 1: Chemical Shift (ppm), Inner Rows and Columns: Intensity (arb. units)
h. FigureS13_PnBATTC.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
i. FigureS14_PnBAH.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
j. FigureS16_Purified2CEAMaterial.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
k. FigureS16_Starting2CEAMaterial.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
l. FigureS17_2CEA1HNMR.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
m. FigureS18_2CEA13CNMR.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
n. FigureS19_PnBA1halfCEATTC.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
o. FigureS20_PnBA1halfCEAH.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
p. FigureS21_PnBA1halfCEAHMethyl.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
q. FigureS23_PnBA1AMPSTTC.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
r. FigureS24_PnBA1AMPSH.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
s. FigureS25_PnBA1AMPSHDioxane.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
t. FigureS26_PnBA1AMPSHMethyl.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
u. FigureS28_PnBA1AMPSEtIm.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
v. FigureS29_PnBA6halfAMPSH.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
w. FigureS29_PnBA6halfAMPSTTC.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
x. FigureS30_PnBA6halfAMPSHDMSO.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
y. FigureS31_PnBA6halfAMPSHMethyl.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
z. FigureS33_PnBA6halfAMPSEtIm.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
aa. FigureS37_1Im1halfCEABlend.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
ab. FigureS38_1Im1AMPSBlend.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
ac. FigureS39_6halfblendsupernantant.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)
ad. FigureS40_6halfblendLiTFSI.csv
1. Variables: Chemical Shift [ppm], Intensity [arb. units]
2. Column names: Chemical Shift (ppm), Intensity (arb. units)E. FiguresS3,S9,S15,S22,S27,S32: Size-exclusion chromatograms of synthesized polymers
a. FigureS3_PDMSPVMS.csv
1. Variables: Elution Time [min], Normalized Intensity [Unitless]
2. Column names: Elution_Time_PDMS (min), Normalized_Intensity_PDMS, Elution_Time_PDMS_1PVMS (min), Normalized_Intensity_PDMS_1PVMS, Elution_Time_PDMS_7PVMS (min), Normalized_Intensity_PDMS_7PVMS
b. FigureS9_PDMSIm.csv
1. Variables: Elution Time [min], Normalized Intensity [Unitless], Intensity [arb. units]
2. Column names: Elution_Time_PDMS_1Im (min), Normalized_Intensity_PDMS_1Im, Elution_Time_PDMS_6halfIm (min), Intensity_PDMS_6halfIm
c. FigureS15_PnBA.csv
1. Variables: Elution Time [min], Normalized Intensity [Unitless]
2. Column names: Elution_Time_PnBA (min), Normalized_Intensity_PnBA
d. FigureS22_PnBA1halfCEA.csv
1. Variables: Elution Time [min], Normalized Intensity [Unitless]
2. Column names: Elution_Time_PnBA_1halfCEA (min), Normalized_Intensity_PnBA_1halfCEA
e. FigureS27_PnBA1AMPS.csv
1. Variables: Elution Time [min], Normalized Intensity [Unitless]
2. Column names: Elution_Time_PnBA_1AMPS (min), Normalized_Intensity_PnBA_1AMPS
f. FigureS32_PnBA6halfAMPS.csv
1. Variables: Elution Time [min], Normalized Intensity [Unitless]
2. Column names: Elution_Time_PnBA_6halfAMPS (min), Normalized_Intensity_PnBA_6halfAMPSF. FiguresS10,S34,S41: Fourier-transform infrared spectra of synthesized polymers and blends
a. FigureS10_PDMS.csv
1. Variables: Wavenumber [cm–1], Normalized Absorbance [unitless]
2. Column names: Wavenumber_PDMS (cm–1), Normalized_Absorbance_PDMS, Wavenumber_PDMS_1Im (cm–1), Normalized_Absorbance_PDMS_1Im, Wavenumber_PDMS_6halfIm (cm–1), Normalized_Absorbance_PDMS_6halfIm
b. FigureS34_PnBA.csv
1. Variables: Wavenumber [cm–1], Normalized Absorbance [unitless]
2. Column names: Wavenumber_PnBA (cm–1), Normalized_Absorbance_PnBA, Wavenumber_PnBA_1halfCEA (cm–1), Normalized_Absorbance_PnBA_1halfCEA, Wavenumber_PnBA_1AMPS (cm–1), Normalized_Absorbance_PnBA_1AMPS, Wavenumber_PnBA_6halfAMPS (cm–1), Normalized_Absorbance_PnBA_6halfAMPS
c. FigureS41a_COOHImBlend.csv
1. Variables: Wavenumber [cm–1], Normalized Absorbance [unitless]
2. Column names: Wavenumber_PnBA_1halfCEA (cm–1), Normalized_Absorbance_PnBA_1halfCEA, Wavenumber_PDMS_1Im (cm–1), Normalized_Absorbance_PDMS_1Im, Wavenumber_ImCOOH_Blend (cm–1), Normalized_Absorbance_ImCOOH_Blend
d. FigureS41b_1SO3HImBlend.csv
1. Variables: Wavenumber [cm–1], Normalized Absorbance [unitless]
2. Column names: Wavenumber_PnBA_1AMPS (cm–1), Normalized_Absorbance_PnBA_1AMPS, Wavenumber_PDMS_1Im (cm–1), Normalized_Absorbance_PDMS_1Im, Wavenumber_1SO3HIm_Blend (cm–1), Normalized_Absorbance_1SO3HIm_Blend
e. FigureS41c_6halfSO3HImBlend.csv
1. Variables: Wavenumber [cm–1], Normalized Absorbance [unitless]
2. Column names: Wavenumber_PnBA_6halfAMPS (cm–1), Normalized_Absorbance_PnBA_6halfAMPS, Wavenumber_PDMS_6halfIm (cm–1), Normalized_Absorbance_PDMS_6halfIm, Wavenumber_6halfSO3HIm_Blend (cm–1), Normalized_Absorbance_6halfSO3HIm_BlendG. FiguresS11,S35,S42: Differential scanning thermograms of synthesized polymers and blends
a. FigureS11_PDMS.csv
1. Variables: Temperature [°C], Normalized Heat Flow [W/g]
2. Column names: Temperature_PDMS (°C), Normalized_Heat_Flow_PDMS (W/g), Temperature_PDMS_1Im (°C), Normalized_Heat_Flow_PDMS_1Im (W/g), Temperature_PDMS_6halfIm (°C), Normalized_Heat_Flow_PDMS_6halfIm (W/g)
b. FigureS35_PnBA.csv
1. Variables: Temperature [°C], Normalized Heat Flow [W/g]
2. Column names: Temperature_PnBA (°C), Normalized_Heat_Flow_PnBA (W/g), Temperature_PnBA_1halfCEA (°C), Normalized_Heat_Flow_PnBA_1halfCEA (W/g), Temperature_PnBA_1AMPS (°C), Normalized_Heat_Flow_PnBA_1AMPS (W/g), Temperature_PnBA_6halfAMPS (°C), Normalized_Heat_Flow_PnBA_6halfAMPS (W/g)
c. FigureS42a_COOHImBlend.csv
1. Variables: Temperature [°C], Normalized Heat Flow [W/g]
2. Column names: Temperature_PnBA_1halfCEA (°C), Normalized_Heat_Flow_PnBA_1halfCEA (W/g), Temperature_PDMS_1Im (°C), Normalized_Heat_Flow_PDMS_1Im (W/g), Temperature_ImCOOH_Blend (°C), Normalized_Heat_Flow_ImCOOH_Blend (W/g)
d. FigureS42b_1SO3HImBlend.csv
1. Variables: Temperature [°C], Normalized Heat Flow [W/g]
2. Column names: Temperature_PnBA_1AMPS (°C), Normalized_Heat_Flow_PnBA_1AMPS (W/g), Temperature_PDMS_1Im (°C), Normalized_Heat_Flow_PDMS_1Im (W/g), Temperature_1SO3HIm_Blend (°C), Normalized_Heat_Flow_1SO3HIm_Blend (W/g)
e. FigureS42c_6halfSO3HImBlend.csv
1. Variables: Temperature [°C], Normalized Heat Flow [W/g]
2. Column names: Temperature_PnBA_6halfAMPS (°C), Normalized_Heat_Flow_PnBA_6halfAMPS (W/g), Temperature_PDMS_6halfIm (°C), Normalized_Heat_Flow_PDMS_6halfIm (W/g), Temperature_6halfSO3HIm_Blend (°C), Normalized_Heat_Flow_6halfSO3HIm_Blend (W/g)H. FiguresS12,S36,S49-51: Small-amplitude oscillatory shear rheological master curves and shift factors of synthesized polymers and blends
a. FigureS12a_PDMSmastercurves.csv
1. Variables: Reduced Frequency [rad/s], Storage Modulus [Pa], Loss Modulus [Pa]
2. Column names: waT_PDMS (rad/s), G'_PDMS (Pa), G''_PDMS (Pa), waT_PDMS_1Im (rad/s), G'_PDMS_1Im (Pa), G''_PDMS_1Im (Pa), waT_PDMS_6halfIm (rad/s), G'_PDMS_6halfIm (Pa), G''_PDMS_6halfIm (Pa)
b. FigureS12b_PDMSshiftfactors.csv
1. Variables: Temperature–Reference Temperature [C], Log(Shift Factor) [unitless]
2. Column names: T-Tref_PDMS (°C), log(aT)_PDMS, T-Tref_PDMS_1Im (°C), log(aT)_PDMS_1Im, T-Tref_PDMS_6halfIm (°C), log(aT)_PDMS_6halfIm
c. FigureS36a_PnBAmastercurves.csv
1. Variables: Reduced Frequency [rad/s], Storage Modulus [Pa], Loss Modulus [Pa]
2. Column names: waT_PnBA (rad/s), G'_PnBA (Pa), G''_PnBA (Pa), waT_PnBA_1halfCEA (rad/s), G'_PnBA_1halfCEA (Pa), G''_PnBA_1halfCEA (Pa), waT_PnBA_1AMPS (rad/s), G'_PnBA_1AMPS (Pa), G''_PnBA_1AMPS (Pa), waT_PnBA_6halfAMPS (rad/s), G'_PnBA_6halfAMPS (Pa), G''_PnBA_6halfAMPS (Pa)
d. FigureS36b_PnBAshiftfactors.csv
1. Variables: Temperature–Reference Temperature [C], Log(Shift Factor) [unitless]
2. Column names: T-Tref_PnBA (°C), log(aT)_PnBA, T-Tref_PnBA_1halfCEA (°C), log(aT)_PnBA_1halfCEA, T-Tref_PnBA_1AMPS (°C), log(aT)_PnBA_1AMPS, T-Tref_PnBA_6halfAMPS (°C), log(aT)_PnBA_6halfAMPS
e. FigureS49_6halfcomparison.csv
1. Variables: Frequency [rad/s], Storage Modulus [Pa], Loss Modulus [Pa]
2. Column names: w_parent_90C, G'_parent_90C, G''_parent_90C, w_blend_90C, G'_blend_90C, G''_blend_90C, w_parent_80C, G'_parent_80C, G''_parent_80C, w_blend_80C, G'_blend_80C, G''_blend_80C, w_parent_70C, G'_parent_70C, G''_parent_70C, w_blend_70C, G'_blend_70C, G''_blend_70C, w_parent_60C, G'_parent_60C, G''_parent_60C, w_blend_60C, G'_blend_60C, G''_blend_60C, w_parent_50C, G'_parent_50C, G''_parent_50C, w_blend_50C, G'_blend_50C, G''_blend_50C, w_parent_40C, G'_parent_40C, G''_parent_40C, w_blend_40C, G'_blend_40C, G''_blend_40C, w_parent_30C, G'_parent_30C, G''_parent_30C, w_blend_30C, G'_blend_30C, G''_blend_30C, w_parent_20C, G'_parent_20C, G''_parent_20C, w_blend_20C, G'_blend_20C, G''_blend_20C
f. FigureS50a_1molblendoriginal.csv
1. Variables: Frequency [rad/s], Storage Modulus [Pa], Loss Modulus [Pa]
2. Column names: w (rad/s), G'_50C (Pa), G''_50C (Pa), w (rad/s), G'_50C_Post_Cool (Pa), G''_50C_Post_Cool (Pa), w (rad/s), G'_50C_Post_Heat (Pa), G''_50C_Post_Heat (Pa), w (rad/s), G'_55C (Pa), G''_55C (Pa), w (rad/s), G'_60C (Pa), G''_60C (Pa), w (rad/s), G'_65C (Pa), G''_65C (Pa), w (rad/s), G'_70C (Pa), G''_70C (Pa), w (rad/s), G'_75C (Pa), G''_75C (Pa), w (rad/s), G'_80C (Pa), G''_80C (Pa), w (rad/s), G'_85C (Pa), G''_85C (Pa), w (rad/s), G'_90C (Pa), G''_90C (Pa), w (rad/s), G'_95C (Pa), G''_95C (Pa), w (rad/s), G'_100C (Pa), G''_100C (Pa), w (rad/s), G'_105C (Pa), G''_105C (Pa), w (rad/s), G'_110C (Pa), G''_110C (Pa), w (rad/s), G'_115C (Pa), G''_115C (Pa), w (rad/s), G'_120C (Pa), G''_120C (Pa)
g. FigureS50b_1molblendrecasted.csv
1. Variables: Frequency [rad/s], Storage Modulus [Pa], Loss Modulus [Pa]
2. Column names: w (rad/s), G'_50C (Pa), G''_50C (Pa), w (rad/s), G'_50C_Post_Heat (Pa), G''_50C_Post_Heat (Pa), w (rad/s), G'_55C (Pa), G''_55C (Pa), w (rad/s), G'_60C (Pa), G''_60C (Pa), w (rad/s) G'_65C (Pa), G''_65C (Pa), w (rad/s), G'_70C (Pa), G''_70C (Pa), w (rad/s), G'_75C (Pa), G''_75C (Pa), w (rad/s), G'_80C (Pa), G''_80C (Pa), w (rad/s), G'_85C (Pa), G''_85C (Pa), w (rad/s), G'_90C (Pa), G''_90C (Pa), w (rad/s), G'_95C (Pa), G''_95C (Pa), w (rad/s), G'_100C (Pa), G''_100C (Pa), w (rad/s), G'_105C (Pa), G''_105C (Pa), w (rad/s), G'_110C (Pa), G''_110C (Pa), w (rad/s), G'_115C (Pa), G''_115C (Pa), w (rad/s), G'_120C (Pa), G''_120C (Pa)
h. FigureS51_6halfmolblend.csv
1. Variables: Frequency [rad/s], Storage Modulus [Pa], Loss Modulus [Pa]
2. Column names: w (rad/s), G'_50C (Pa), G''_50C (Pa), w (rad/s), G'_60C(Pa), G''_60C (Pa), w (rad/s), G'_60C_Post_Cool (Pa), G''_60C_Post_Cool (Pa), w (rad/s), G'_60C_Post_Heat (Pa), G''_60C_Post_Heat (Pa), w (rad/s), G'_70C (Pa), G''_70C (Pa), w (rad/s), G'_80C (Pa), G''_80C (Pa), w (rad/s), G'_90C (Pa), G''_90C (Pa), w (rad/s), G'_100C (Pa), G''_100C (Pa), w (rad/s), G'_110C (Pa), G''_110C (Pa), w (rad/s), G'_120C (Pa), G''_120C (Pa)I: FiguresS43-46,S48: Small angle X-ray scattering patterns of synthesized polymers and blends at room temperature, or elevated temperatures.
a. FigureS43a_1SO3HImBlend.csv
1. Variables: Scattering Wavevector [A-1], Intensity [arb. units]
2. Column names: q_PnBA_1AMPS (A-1), I_PnBA_1AMPS (arb. units), q_PDMS_1Im (A-1), I_PDMS_1Im (arb. units), q_1SO3HIm_Blend (A-1), I_1SO3HIm_Blend (arb. units)
b. FigureS43b_6halfSO3HImBlend.csv
1. Variables: Scattering Wavevector [A-1], Intensity [arb. units]
2. Column names: q_PnBA_6halfAMPS (A-1), I_PnBA_6halfAMPS (arb. units), q_PDMS_6halfIm (A-1), I_PDMS_6halfIm (arb. units), q_6halfSO3HIm_Blend (A-1), I_6halfSO3HIm_Blend (arb. units)
c. FigureS44a_1SO3HImBlendR1.csv
1. Variables: Scattering Wavevector [A-1], Intensity [arb. units]
2. Column names: q_Pristine (A-1), I_Pristine (arb. units), q_1_Month (A-1), I_1_Month (arb. units), q_3_Months (A-1), I_3_Months (arb. units)
d. FigureS44b_1SO3HImBlendR2.csv
1. Variables: Scattering Wavevector [A-1], Intensity [arb. units]
2. Column names: q_Pristine (A-1), I_Pristine (arb. units), q_1_Month (A-1), I_1_Month (arb. units)
e. FigureS45_1SO3HImBlendR1VT.csv
1. Variables: Scattering Wavevector [A-1], Intensity [arb. units]
2. Column names: q_25C (A-1), I_25C (arb. units), q_50C (A-1), I_50C (arb. units), q_70C (A-1), I_70C (arb. units), q_90C (A-1), I_90C (arb. units), q_100C (A-1), I_100C (arb. units), q_110C (A-1), I_110C (arb. units), q_120C (A-1), I_120C (arb. units), q_130C (A-1), I_130C (arb. units), q_140C (A-1), I_140C (arb. units), q_150C (A-1), I_150C (arb. units), q_140C_Cool (A-1), I_140C_Cool (arb. units), q_130C_Cool (A-1), I_130C_Cool (arb. units), q_120C_Cool (A-1), I_120C_Cool (arb. units), q_100C_Cool (A-1), I_100C_Cool (arb. units), q_90C_Cool (A-1), I_90C_Cool (arb. units), q_70C_Cool (A-1), I_70C_Cool (arb. units), q_50C_Cool (A-1), I_50C_Cool (arb. units), q_25C_Cool (A-1), I_25C_Cool (arb. units)
f. FigureS46_1SO3HImBlendR2VT.csv
1. Variables: Scattering Wavevector [A-1], Intensity [arb. units]
2. Column names: q_25C (A-1), I_25C (arb. units), q_50C (A-1), I_50C (arb. units), q_70C (A-1), I_70C (arb. units), q_90C (A-1), I_90C (arb. units), q_100C (A-1), I_100C (arb. units), q_110C (A-1), I_110C (arb. units), q_120C (A-1), I_120C (arb. units), q_130C (A-1), I_130C (arb. units), q_140C (A-1), I_140C (arb. units), q_150C (A-1), I_150C (arb. units), q_140C_Cool (A-1), I_140C_Cool (arb. units), q_130C_Cool (A-1), I_130C_Cool (arb. units), q_120C_Cool (A-1), I_120C_Cool (arb. units), q_100C_Cool (A-1), I_100C_Cool (arb. units), q_90C_Cool (A-1), I_90C_Cool (arb. units), q_70C_Cool (A-1), I_70C_Cool (arb. units), q_50C_Cool (A-1), I_50C_Cool (arb. units), q_25C_Cool (A-1), I_25C_Cool (arb. units)
g. FigureS48_1SO3HImBlendRecast.csv
1. Variables: Scattering Wavevector [A-1], Intensity [arb. units]
2. Column names: q_Post_VT (A-1), I_Post_VT (arb. units), q_Recasted (A-1), I_Recasted (arb. units)J: FigureS47: Domain size as a function of temperature for 1 mol% blend
a. FigureS47_1molblendVTdomainR2.csv
1. Variables: Temperature [°C], Primary Peak Wavevector [A-1], Domain Size [nm]
2. Column names: T (°C), q* (A–1), d (nm) -
Relationship between files, if important: N/A
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Additional related data collected that was not included in the current data package: N/A
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Are there multiple versions of the dataset? No
METHODOLOGICAL INFORMATION
- Description of methods used for collection/generation of data: Please refer to supporting information document for methodology of data generation and collection.
- Methods for processing the data: Please refer to supporting information document for methodology of data processing.
- Instrument- or software-specific information needed to interpret the data: N/A
- Standards and calibration information, if appropriate: Molecular weight values reported from size-exclusion chromatography measurements were calibrated to known poly(styrene) standards with known molecular weights.
- Environmental/experimental conditions: N/A
- Describe any quality-assurance procedures performed on the data: N/A
- People involved with sample collection, processing, analysis and/or submission: Jerrick Edmund, Kseniia M. Karnaukh, Shuyi Xie, Elizabeth A. Murphy, Allison Abdilla, Eiko Ino, Javier Read de Alaniz, Craig J. Hawker, Rachel A. Segalman